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General procedure for synthesis of 11-X-MG derivatives (1517) Starting material ( 5 , 7 , or 13 , 0.11 mmol) was dissolved in AcOH (2.0 mL) under argon and NaBH 3 CN (13.7 mg, 0.22 mmol, 2 equiv.) was added to the solution

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Instances of contamination and improper dosing are not uncommon, and the consequences can be severe

doi: 10.1016/0016-5085(91)90094-2

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