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The mass spectrometer was operated with a drying gas temperature of 325 C with a flow rate of 13 L/min, sheath gas temperature of 275 C with a flow rate of 12 L/min, nebulizer pressure at 45 psi, and capillary voltage set at + 4000 V/3000 V

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Subsequent in vitro studies testing the analytic measurement range and linearity of the DOACs (Figure 3) showed a strong linear dose response across the tested concentration ranges with R2 values of 0.9705 to 0.9863 for the three DOACs and precision values ranging between 0.85 3.84 CVs

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